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A new polymorph of the copper(II) thiocyanate complex with 2-dimethylaminoethanol, [Cu 2 (Me 2 Ea) 2 (NCS) 2 ] ∞  (HMe 2 Ea = 2-dimethylaminoethanol, HL) 1, was isolated in the attempted synthesis of a mixed-metal complex from zerovalent copper, cadmium oxide and ammonium thiocyanate in CH 3 CN solution of HL in air. [Cu 2 (Me 2 Ea) 2 (NCS) 2 (DMSO) 2 ]  2  is a product of recrystallization of 1 from DMSO. X-ray analysis carried out on single crystals for both compounds revealed that 1 is a rare example of a 1D coordination polymer consisting of two chains in which the metallic centres are connected through single end-to-end NCS groups. The chains are inter-linked through alkoxo-bridges of L groups between the neighboring copper atoms. Complex 2 is a centrosymmetric dimer composed of two CuL(NCS)DMSO units linked by alkoxo-bridges of L groups.

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Polymeric Double [Cu(NCS)] Chains in the Crystal Structure of [Cu 2 (Me 2 Ea) 2 (SCN) 2 ] ∞  (HMe 2 Ea = 2-Dimethylaminoethanol) (NewP olymorph) and the Dimeric Structure of its DMSO Adduct