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An excellent supersilylation agent, supersilyl triflate, tBu 3 SiO 3 SCF 3 , is easily obtained from tBu 3 SiH and CF 3 SO 3 H. Supersilyl triflate, tBu 3 SiO 3 SCF 3 , reacts with lithium amide or lithium hydrazide to form the supersilyl amine, tBu 3 SiNH 2 , or the supersilyl hydrazines, tBu 3 SiNHNH 2  and tBu 3 SiNH-HNSitBu 3 , respectively. The structures of supersilyl triflate, tBu 3 SiO 3 SCF 3 , and bissupersilyl hydrazine, tBu 3 SiNH-HNSitBu 3 , have been determined by X-ray structure analysis.

zeitschrift für naturforschung b

Supersilyliertes Ammoniak und supersilyliertes Hydrazin: Synthese, Struktur und Eigenschaften / Supersilyl Ammonia and Supersilyl Hydrazine: Synthesis, Structure and Properties