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The structures of the compounds [Rh(bpy) 2 (py)(Cl)](ClO 4  ) 2  (2 (ClO 4  ) 2 ) and [Rh(phen) 2 (py)- (Cl)](ClO 4  ) 2  (7 -(ClO 4  ) 2 ) were determined by single-crystal X-ray diffraction. Both complexes show a six-coordinate rhodium atom with two bpy or phen ligands in the cis configuration. The Rh-Cl distances are 2.334(3) and 2.323(2) Å, respectively. The bond angles N-Rh-Cl formed with the axially-positioned nitrogen atom are 174.4(2) and 173.8(2)°. The oxidation of aquo complexes, prepared from the corresponding rhodium chloride complexes, by two equivalents of Ce(IV) in 60% HCIO 4  solution yields the corresponding mono-oxo products. All complexes have been identified and characterized by elemental analyses, IR, and  1 H NMR data

Structural Characterization Of Rh(Iii) Complexes Containing The Polypyridyl Ligands And Some Properties Of Their Derivatives