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Water- and oxygen-sensitive compounds of the type R ’ n EHal 3-n  (R' = SitBu 2 Ph; E = Triel) with or without donors, viz. RAlBr 2 , R' 3 Al, R'GaCl 2 'THF, R'GaCl 2 , R' 3 Ga, R'InCl 2 ·THF and R' 3 In have been synthesized by reaction of EX 3  with NaSitBu 2 Ph (prepared for this purpose) in the absence or presence of donors. The dihalides R'EHal 2  have also been obtained by reaction of R' 3 E with EHal 3 , whereas monohalides R' 2 EHal are not accessible via these and other routes up to date. All trielanes have been characterized by NMR and the structures of the R' 3 E compounds have been determined by X-ray analyses.

zeitschrift für naturforschung b

Silyltrielane R'  n Hal 3-n  (E = Al, Ga, In; R' = SitBu 2 Ph): Synthesen, Charakterisierung, Strukturen [1] / Silyltrielanes R' n EHal 3-n  (E = Al, Ga, In; R' = SitBu 2 Ph): Syntheses, Characterization, Structures [1]