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Cbz protected α-aminonitriles 1 or α-aminocarboxamides 2 were converted to imidates 3 either by Pinner reaction or by Meerwein’s reagent. Sulfhydrolysis of 3 produced α-aminothiocarboxylic O-esters 4 which in turn were reacted with hydroxylamine to give Cbz protected (E)-α-aminocarbohydroximic esters 5. Hydrogenolysis of 5 furnished the target compounds 6 .

Synthese und Eigenschaften von α Aminocarbohydroximsäure-estern / Synthesis and Properties of α-Aminocarbohydroximic Esters