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The acid-labile 5-[(9-aminoxanthen-2-yl)oxy]valeric acid was prepared in a six-step route. The usefulness of the resulting handle was investigated with solid-phase peptide synthesis of cholecystokinin-8 sulfate and the phosphorylated fragment of the ζ-subunit of the T-cell receptor complex 138-144.

Synthesis and Solid-Phase Application of a 9-Xanthenyl Handle