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Four differently methyl-substituted tetraphenyl imidodiphosphates [(H 3 C)nC 6 H 5-n ] 2 PO-NH-PO[C 6 H 5-n (C 3 ) n ] (n = 1, 2), i. e. the 4-, 3,4-, 3,5-and 2,3-derivatives, have been crystallized and their structures determined to gain information on the spatial requirements as ligands in the corresponding cesium salts. According to the packing coefficients calculated from the structural data, they increase in the sequence 4&lt;3,5&lt;3,4&lt;2,3. The most perturbed structural motif is the hydrogen bonded, eight-membered of each the dimer subunits.

zeitschrift für naturforschung b

Wechselwirkungen in Molekülkristallen, 174 [1, 2]. Kristallzüchtung und Strukturbestimmung verschiedenartig Methyl-substituierter Imidodiphosphorsäuretetraphenylester / Interaction in Molecular Crystals, 174 [1, 2]. Crystal Growth and Structure Determination of Differently Methyl-Substituted Tetraphenyl Imidodiphosphates