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The solid state synthesis and the crystal structure of Cs 6 Cl 4 O(Pearson-code hR22, R3c, a = 1324.7(6), c = 1658(1) pm, Z = 6, 931 reflections with I o  &gt; 2σ(I), R 1  = 0.040, wR 2  = 0.114) are reported. The compound crystallises isotypically with Rb 6 Cl 4 O in the anti-K 4 CdCl 6  type of structure. The structure consists of infinite chains of alternating face-sharing OCs 6  octahedra and ClCs 6  trigonal prisms which are separated by chloride anions. The underlying structural concept and the analogy to perovskites are outlined.

Darstellung und Kristallstruktur von Cs 6 Cl 4 O / Preparation and Crystal Structure of Cs 6 Cl 4 O