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The tris(alkinyl)phosphine complexes {(PhC=C) 3 P} 3 M(CO) 3 , M = Cr (3a), Mo (3b), W (3c), are obtained from P(C=CPh) 3  and (C 6 H 15 N 3 )M(CO) 3  (C 6 H 15 N 3  = 1,3,5-trimethyl-1,3,5-triazacyclohexane) as stable yellow solids in good yields. While IR data indicate significant acceptor properties of the phosphane ligands, the X-ray structure analysis of 3c also allows the discussion of weak donor interactions.

Über Komplexe des Typs {(PhC=C) 3 P} 3 M(CO) 3 (M = Cr, Mo, W) / On Complexes of the Type {(PhC=C) 3 P} 3 M(CO) 3 (M = Cr, Mo, W)