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Thioantimonates, Solvothermal Synthesis, Chalcogenides The reaction of elemental manganese, antimony and sulfur with ethylamine under mild solvothermal conditions yielded a thioantimonate(III) with composition Mn 2 (EA) 2 Sb 2 S 5  (EA = C 2 H 5 NH 2 ) that is a new member of a series of polymeric manganese thioantimo-nates(III). The structure of the title compound consists of layers of a neutral mesh-like Mn2Sb2S5 framework. The ethylamino ligands coordinated to the Mn centres separate the sheets and fill the voids within the layers formed by the interconnection of Mn 2 Sb 2 S 4  hetero-cubane like building blocks. Below 273 K a reversible phase transition occurs, which is accom­panied by a doubling of the crystallographic a-axis.

Synthesis and Crystal Structure of Mn 2 (C 2 H 5 NH 2 ) 2 Sb 2 S 5 Exhibiting a Reversible Phase Transition