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The cationic thorium(IV) complexes [Th{Ph 2 P(O)CH 2 CH 2 P(O)Ph 2 } 2 (NO 3 ) 3 ]NO 3  and [Th{Ph 2 P(O)NP(O)Ph 2 } 3 (dmso) 2 ]NO 3  have been synthesized by reactions of Th(NO 3 ) 4  · 5H 2 O with bis(diphenylphosphino)ethane dioxide, Ph 2 P(O)CH 2 CH 2 P(O)Ph 2  (L 1 ), or ammonium bis(diphenylphosphoryl)amide, (NH 4 )[Ph 2 P(O)NP(O)Ph 2 ] (NH 4 L 2 ), and subsequent recrystallization from dimethyl sulfoxide. The products have been studied spectroscopically and by X-ray crystallography.

zeitschrift für naturforschung b

Syntheses and Structures of Thorium(IV) Complexes with Bis(diphenylphosphino)ethane Dioxide, Ph 2 P(O)CH 2 CH 2 P(O)Ph 2 , and Bis(diphenylphosphoryl)amide, [Ph 2 P(O)NP(O)Ph 2 ]