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Depending on the reaction conditions methylaluminium dichloride, MeAlCl 2 , and trimethylsilyl alkanethiolates, Me 3 SiSR, give dichloroaluminium alkanethiolates, Cl 2 AlSR with R = Me and Et or methylchloroaluminium alkanethiolates, MeAl(SR)Cl with R = Me, Et, and i-Pr. The reaction pathways are described and IR and  1 H NMR spectroscopic data are presented.

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Formation of Methylchloroaluminium Alkanethiolates, MeAl(SR)Cl, and Dichloroaluminium Alkanethiolates, Cl 2 AlSR, from Methylaluminium Dichloride and Trimethylsilyl Alkanethiolates, Me 3 SiSR