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Reaction of tetramethylcyclopentenone and cyclopentadienyl anion gave the title pentafulvalene derivative. Its deprotonation with sodium or potassium hydride proceeded selectively at one of the methyl groups. The resulting 3,4-dihydro-1,3,4-trimethyl(2-methylene)pentafulvalenide ion was converted to the corresponding ferrocene which was obtained as two diasteroisomers in the ratio of 1/1.

3.4-D ihydro-1, 2, 3, 4-tetramethyl- pentafulvalene and its Conversion to Ferrocenes