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Treatment of the spacer modified glucose derivative 1 with diethylaminotrimethylsilane furnished the bis-silylated molecule 2. Reaction of 2 with two equivalents of the phosphorus compounds 3, 4, and 5 led to the spacer phosphorylated glucosyl derivatives 6, 7 and 8. Complexation of 6 with (COD)PtCl 2  gave complex 9; the cis-conformation of 9 could be confirmed by  31 P NMR investigations

zeitschrift für naturforschung b

Synthese und Komplexierung Phosphorylierter spacer-modifizierter Glucosederivate/ Synthesis and Complexation of Spacer Modified Phosphorylated Glucose Derivatives