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Lithium Phosphides, Cyclopentadienides Treatment of 6,6-dimethylfulvene with LiPHPh in hexane/TMEDA (TMEDA = N,N,N′,N′- tetramethylethylenediamine) affords the monolithiated phosphinomethyl cyclopentadienide [Li(TMEDA)][PhHPCMe 2 C 5 H 4 ] (1). Further reaction with Li n Bu in diethylether/TMEDA leads to the formation of the doubly lithiated phosphidomethyl cyclopentadienide [Li(TMEDA)] 2 [PhPCMe 2 C 5 H 4 ] (2) whose crystal and molecular structure was determined (orthorhombic, space group P2 1 2 1 2 1 , a = 9.579(4), b = 12.788(2), c = 24.108(6) Å, Z = 4)

Polylithiation of Small Molecules. Synthesis and Structure of the Functional Lithium Phosphide [Li(TMEDA)] 2 [PhPCMe 2 C 5 H 4 ]