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By reaction of hexamethyldisilazane with aluminium trichloride in hexane hexamethyldisilazane-trichloroaluminum [(H 3 C) 3 Si] 2 NH • AlCl 3  is formed. The adduct has been characterized by MS, IR, Raman,  1 H,  13 C,  27 Al,  29 Si NMR spectroscopy, and by a crystal structure determination (1425 independent reflections, R = 0.035). The space group is Pbca with a = 1312,6(5), b = 1182,9(5), c = 1964,7(5) pm; Z = 8. [(H 3 C) 3 Si] 2 NH • AlCl 3  forms monomeric units which have point symme­try C 1  and exhibit an Al − N bond length of 193,9(3) pm.

zeitschrift für naturforschung b

Kristallstruktur und spektroskopische Charakterisierung von Hexamethyl- disilazan-Aluminiumtrichlorid [(H 3 C) 3 Si] 2 NH ∙ AlCl 3  /  Crystal Structure and Spectroscopic Characterisation of Hexamethyl- disilazane-trichloroalum inum [(H 3 C) 3 Si] 2 NH ∙ AlCl 3