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By careful oxidation of trans-tetrafluorodichloroosmate(IV) with PbO 2 /trifluoroacetic acid in dichloromethane the corresponding osmium(V) complex anion rran5 -[OsF 4 Cl 2 ] -  is for­ med. The X-ray structure determination on a single crystal has been performed of trans-(Et 4 N)[OsF 4 Cl 2 ] (triclinic, space group P1̄a = 7.190(5), b = 7.205(5), c = 7.732(5) Å, a = 71.28(1), β = 71.32(1), 7 = 70.76(1)°, Z = 1). Based on the molecular parameters of the X-ray determination the IR and Raman spectra of the complex have been assigned by normal coordi­ nate analysis. The valence force constants are: f d (OsCl) = 2.13 and f d (OsF) = 3.81 mdyn/Å.

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Kristallstruktur, Schwingungsspektren und Normalkoordinatenanalyse von trans-(Et 4 N)[OsF 4 Cl 2 ] / Crystal Structure, Vibrational Spectra and Normal Coordinate Analysis of trans-(Et 4 N)[OsF 4 Cl 2 ]