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A new strategy for the asymmetric syntheses of polysubstituted pyrano-furanoids using allylic sulfates derived from carbohydrate precursors and the dianion of diethoxycarbonyl acetone, catalyzed by Pd(0), is described.

Carbohydrates to Pyrano-Furanoids: New and Regioselective Palladium-Catalyzed Syntheses of Tetrasubstituted Furanoids from Carbohydrate Scaffolds