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The syntheses of different nitroxide radicals are reported. The thermal behaviour of the ni­ troxide radicals was examined by polarizing microscopy, differential scanning calorimetry as well as X-ray diffraction experiments. Temperature dependent magnetic susceptibility mea­surements were carried out in order to determine the magnetic properties of these nitroxide radicals. The majority of the radicals presented here show weak antiferromagnetic exchange interactions.

zeitschrift für naturforschung b

Darstellung und magnetische Eigenschaften einiger kristalliner Nitroxidradikale/Synthesis and Magnetic Properties of Some Crystalline Nitroxide Radicals