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The reaction of arsenic, MgSO 4  and S 2 Cl 2  in acetonitrile yielded the title compound along with 4,5- dichloro-1 ,2,3-dithiazolium chloride, [C 2 NS 2 Cl 2 ]Cl (which was formed from the solvent and S 2 Cl 2 ). The crystal strucutre of [Mg(NCCH 3 ) 6 ][As 4 Cl 14 ] was determined by X-ray diffraction. It is triclinic, space group P1¯, Z = 2, R = 0.049. The Mg 2+  ion is coordinated by six acetonitrile ligands. The anions consist of AsCl 4 - and AsCl 3  units which are associated to chains along the a axis by As ··· Cl contacts. Each As atom has distorted octahedral coordination.

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Zu Strängen assoziierte Ionen [AsCl 4 · AsCl 3 ] -  im [Mg(NCCH 3 ) 6 ][As 4 Cl 14 ] / Strands of Associated [AsCl 4 · AsCl 3 ] -  Ions in [Mg(NCCH 3 ) 6 ][As 4 Cl 14 ]