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The reaction of [Ru(tpy)(PPh 3 )(Cl) 2 ] (tpy = 2,2′:6′,2″-terpyridine) with sodium azide in acetone/water afforded [Ru(tpy)(PPh 3 )(N 3 )2]. The new Ru-diazide complex was fully characterized by elemental analysis, IR, Raman, and multinuclear NMR spectroscopy. The structures, energies and vibrational frequencies of the ruthenium diazide isomers, cis- and trans- [Ru(tpy)(PMe 3 )(N 3 ) 2 ] (Me=CH 3 ), were calculated at the semi-empirical ZINDO/1 level of theory.

Synthesis, Spectroscopic Investigation, and Theoretical Study of the Ruthenium Diazide Complex [Ru(tpy)(PPh 3 )(N 3 ) 2 ]