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3,3,5,5-Tetraphenyl-1,2,4-trithiolane (1) reacts with twofold excess of (Ph 3 P) 2 Pt(η 2 -C 2 H 4 ) (4) to give a 1:1 mixture of the complexes (Ph 3 P) 2(6a) and (Ph 3 P) 2 Pt(η 2 -Ph 2 C=S) (7a). Treatment of 3,3,6,6-tetraphenyl-1,2,4,5-tetrathiane (2) with a fourfold excess of 4 yields [Pt 2 (PPh 3 ) 4 (μ-S) 2 ] (8) and the platinum(O) compound 7a. The reaction of the 1,2,3,5,6- pentathiepane 3 with a fourfold excess of 4 affords a 1:1:1 mixture of 8, the platinum(O) complex 7b and the bis-thiolato platinum(II) complex 6b. The thioketone complexes 7a-c were formed in smooth reactions of 4 with the thioketones 5a-c. The molecular structure of (Ph 3 P) 2 Pt(η 2 -Ph 2 C=S) (7a) has been established by single-crystal X-ray analysis.

zeitschrift für naturforschung b

Metallkomplexe mit funktionalisierten Schwefelliganden, XV [1]. Reaktionen von Platin(0)-Komplexen mit 1,2,4-Trithiolanen, 1,2,4,5-Tetrathianen, 1,2,3,5,6-Pentathiepanen sowie Thioketonen. Kristallstrukturanalyse von (Ph 3 P) 2 Pt(η 2 -Ph 2 C=S) / Metal Complexes of Functionalized Sulfur Containing Ligands, XV [1]. Reactions of Platinum(O) Complexes with 1,2,4-Trithiolanes, 1,2,4,5-Tetrathianes, 1,2,3,5,6-Pentathiepanes as well as Thioketones. X-Ray Structure Analysis of (Ph 3 P) 2 Pt(η 2 -Ph 2 C=S)