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Cadmium metal was oxidized in the presence of N-methylisatin N(4)-cyclohexyl-thiosemicarbazone (HMeIs 4 Chex) in an acetonitrile solution, which produced a complex of the formula [Cd(MeIs 4 Chex) 2 ]. The two MeIs 4 Chex ligands are at an angle close to 90° from each other, and there is hydrogen bonding to two adjacent molecules by the anionic ligands remaining NH groups. The complex crystallizes in the monoclinic space group P2 1 /c with a = 11.820(4), b = 11.491(4), c = 27.834(4) Å, β = 106.82(2)°, V = 3618.7(17) Å 3  and Z = 4.

Electrochemical Synthesis of a 6-Coordinate Cadmium(II) Complex with N-Methylisatin N(4)-cyclohexylthiosemicarbazone