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1,1,3,3-Tetrakis(dimethylamino)-1λ 5 ,3λ 5 -diphosphete, (1), reacts with 2-cyano-pyridine to yield 6- pyridyl-1-aza-2λ 5 ,4A 5 -diphosphinine (3). 3 is characterized by its  1 H ,  31 P, and  13 C NMR, mass, and IR spectra as well as the results of the X-ray structure analysis.

6-Pyridyl-1-aza-2λ 5 ,4λ 5 -diphosphinin - ein 2,2′-Bipyridin-Analogon/ 6-Pyridyl-1-aza-2λ 5 ,4λ 5 -diphosphinine - a 2,2′-Bipyridine Analogue