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The chiral orthometallated palladium complex (S)-[Pd{C 6 H 4  (CH(CH 3 )N(CH 3 ) 2  )-C,N}Cl] 2  (1) can be used as a reagent for the determination of the enantiomeric ratio of α-amino acids. By reaction of 1 with mixtures of several D- and L-α-amino carboxylates diastereoisomers of the α-amino acidato complexes 2a - g are obtained.  1 NMR determination of the ratio of the diastereoisomers provides the D/L-ratio of the used D- and L-α-amino carboxylates and is therefore a simple method for the determination of the enantiomeric ratio of α-amino acids.

zeitschrift für naturforschung b

Metallkomplexe mit biologisch wichtigen Liganden, CXXIV [1]. NMR-spektroskopische Bestimmung des Enantiomerenverhältnisses von α-Aminosäuren mit Hilfe eines chiralen orthometallierten Palladiumkomplexes/Metal Complexes of Biologically Important Ligands, CXXIV [1]. NMR-Spectroscopic Determination of the Enantiomeric Ratio of α-Amino Acidsby Use of a Chiral Orthometallated Palladium Complex