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By electrochemical oxidation of (n-Bu 4 N)[B 6 H 5 H fac (CH 2 Ph)] in the presence of nitrite ions in dichloromethane solution cis-[B 6 H 4 (CH 2 Ph)(N O 2 )] 2-  is formed. X-ray diffraction analysis has been performed on a single crystal of cis-(Ph 4 P) 2 [B 6 H 4 (CH 2 Ph)(NO 2 )] HO 2 CH 3 CN (triclinic, space group Pl̅ a = 11.338(5), b = 11.377(5), c = 21.081 (5) Å, α = 93.727(5), ß = 98.872(5), γ = 105.926(5)°, Z = 2). The  11 B NMR spectrum is consistent with a disubstituted octahedral B 6  cage with local C 2v  symmetry. The IR and Raman spectra exhibit characteristic CH, NO 2 , BN, BH and B 6  vibrations.

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Synthese, Spektren und Kristallstruktur von cis-Monobenzylmononitrotetrahydro-closo-hexaborat(2-) / Synthesis, Spectra and Crystal Structure of cis-Monobenzylmononitrotetrahydro-closo-hexaborate(2-)