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Yellow-orange single crystals of [Ph 3 AsBr] 2 [TeBr 6 ] have been prepared from saturated solutions of Ph 3 AsBr 2  and TeBr 4  in acetonitrile and characterized by a crystal structure determination. Space group R3̄c, Z = 12, lattice dimensions at -70 °C: a = b = 1337.9(2), c = 7953.8(4) pm, R = 0.0691. The structure consists of discrete ions [Ph 3 AsBr] +  and nearly perfectly octahedral [TeBr 6 ] 2- .

Die Kristallstruktur von Bis(bromotriphenyl) arsen(V)-hexabromotellurat( IV), [Ph 3 AsBr] 2 [TeBr 6 ]