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The diamagnetic halfsandwich complexes [V(η 7 -C 7 H 7 )(CO) 3 ] and [V(η 5 -L 5 )(CO) 4 ] have been used as intermediates in the conversion of hexcarbonylvanadium, V(CO) 6 , to the paramagnetic trovacene derivatives, [V(η 5 -L 5 )(η 7 -C 7 H 7 )] [L 5  = cyclopentadienyl ligand, C 5 H 4 -R (R = H (1), Me (1a),  t Bu (1b)) and C 5 Me 5  (1c); indenyl (2) and 2-methylindenyl (2a)]. The molecular structure of 2a has been determined: the distances between vanadium and the center Z of the (nearly parallel) ring ligands are 193.0 pm (V-Z 5 ) and 146.2 pm (V-Z 7 ).

Mixed-Sandwich η 5 /η 7 Vanadium Complexes. The Molecular Structure of (η 5 -2-Methyl-indenyl)-(η 7 -cycloheptatrienyl)-vanadium