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By electrochemical oxidation of (n-Bu 4 N)[B 6 H 5 H fac (C 2 H 5 )] in the presence of nitrite ions and of the base DBU in dichloromethane solution cis-[B 6 H 4 (C 2 H 5 )(NO 2 )] 2-  is formed. X-ray diffraction analysis has been performed on a single crystal of cis-(Ph 4  As) 2 [B 6 H 4 (C 2 H 5 )(NO 2 )] (triclinic, space group P1; a = 10.673(4). b = 10.907(4), c = 21.237(4) A, α = 80.789(4), β = 83.117(4), γ = 66.548(2)°, Z = 2). The  11 B NMR spectrum is consistent with a disubstituted octahedral B 6  cage with local Cs symmetry. The IR and Raman spectra exhibit characteristic CH 3 , CH 2 , NO 2 , BN, BH and B 6  vibrations

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Darstellung,  11 B-NMR- und Schwingungsspektren von c/s-Monoethylmononitrotetrahydro- c/050-hexaborat(2-) sowie Kristallstruktur von cis (Ph 4 As) 2 [B 6 H 4 (C 2 H 5 )(NO 2 )] / Synthesis,  11 B NMR and Vibrational Spectra of cis-Monoethylmononitrotetrahydroc-closo-hexaborate(2-) and Crystal Structure of cis-(Ph 4 As) 2 [B 6  H 4  (C 2 H 5  )(NO 2 )]