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The preparation of the first and second generation carbosiloxane dendrimers Si[OCH 2 - CH 2 CH 2  SiMe(OCH 2 C=CH) 2 ] 4  (3) and Si{OCH 2 H 2 CH 2 SiMe[OCH 2 CH 2 CH 2 SiMe(OCH 2  - C=CH) 2 ] 2 } 4  (5) by the reaction o f Si(OCH 2 CH 2 CH 2 SiMeCl 2 ) 4  (1) or Si[OCH 2 CH 2 CH 2 SiMe- (OCH 2 CH 2 CH 2 SiMeCl 2 ) 2 ] 4  (4) with HOCH 2 C =CH (2) in the presence o f NEt 3  is described. Dendrimers 3 and 5 contain propargyloxy units as terminal groups, which can be transferred to Co 2 ((CO) 8  (6) to give the hexacarbonyldicobalt functionalized dendritic molecules Si{OCH 2 CH 2 CH 2 [(η-OCH 2 C=CH)CO 2 (CO) 6 ] 2 } 4  (7) and Si{OCH 2 CH 2 CH 2 SiMe-(OCH 2 CH 2 CH 2 SiMe[(η-OCH 2 C=CH)CO 2 (CO) 6 ] 2 ) 2 } 4  (8).

zeitschrift für naturforschung b

1.2-Verzweigte Carbosiloxan-Dendrimere mit Hauptgruppenelementund Übergangsmetall-modifizierten Oberflächen / 1.2-Branched Carbosiloxane-Dendrimers with Main-Group Element and Transition-Metal Modified Surfaces