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[ i Pr 2 GaN(H) t Bu] 2  (1) and [Mes(Cl)GaN(H) t Bu] 2  (2) can be synthesized by the metathesis reaction of  i Pr 2 GaCl and MesGaCl 2  with one equivalent of LiN(H) t Bu, respectively. 1 and 2 were characterized by NMR, IR and MS techniques as well as by X-ray structure analyses. 1 and 2 consist of centrosymmetric dimeric molecules with a Ga 2 N 2  skeleton. According to cryoscopic measurements in benzene, both amides are dimeric in solution, too.

zeitschrift für naturforschung b

Organogallitimamide: Synthese und Kristallstrukturen von [ i Pr 2 GaN(H) t Bu] 2  und [Mes(Cl)GaN(H) t Bu] 2  / Organogallium Amides: Synthesis and Crystal Structures of [ i Pr 2 GaN(H) t Bu] 2  und [Mes(Cl)GaN(H) t Bu] 2