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Irrespective of the ratio of the reactands AsBr 3  and mesMgBr (mes = mesityl), two products are formed in THF solution: dimesitylarsenic bromide and a magnesium bromoarsenate of composition MgAs 5 Br 17  · n THF. The latter, on crystallization from acetonitrile, yields [Mg(NCMe) 4 (THF) 2 ][As 3 Br 11  ]. The anion of this salt can be described as derived from three face sharing AsBr 6  octahedra. The lone pair of electrons at the As atoms is stereochemically not active.

zeitschrift für naturforschung b

Unerwartete Reaktionsprodukte bei der Umsetzung von Mesitylmagnesiumbromid mit Arsentribromid / Unexpected Products from the Reaction of Mesitylmagnesium Bromide and Arsenic Tribromide