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A series of new ansa-zirconocene dichloride compounds [PR(C 5 H 4 ) 2 ZrCl 2 ; R = Me (5), Et (6),  i Pr (7),  t Bu (8)] with phosphorus as bridging atom between the cyclopentadienyl rings have been prepared, isolated, and characterised by  1 H,  13 C,  31 P NMR spectroscopy, mass spectrometry and elemental analysis. The X-ray structure of 5 is reported.

zeitschrift für naturforschung b

Dichloro[bis(η 5 -2,4-cyclopentadien-l-yl)alkylphosphan]zirconium: PR(C 5 H 4 ) 2 ZrCl 2 ; R = Me, Et,  i Pr,  t Bu / Dichloro[bis(η 5 -2 ,4 -cyclopentadien-l-yl)alkylphosphine]zirconium: PR(C 5 H 4 ) 2 ZrCl 2 ; R = Me, Et,  i Pr,  t Bu