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Single crystals of Fe[B 2 P 2 O 7 (OH) 5 ] were grown under hydrothermal conditions at 170 °C. The crystal structure (monoclinic, C 2/c (Nr. 15), a = 1774.7(5), b = 672.0(2), c = 705.9(2) pm, β = 109.01(2)°, Z = 4, D x = 2.808 g/cm 3 ) contains vierereinfach tetrahedral chains  1  ∞ [B 2 P 2 O 7 (OH) 5 ] 3- , which are formed by alternating borate and phosphate groups connected via common corners:  1  ∞ [BO 2/2 (OH)(OH 0.5 )-PO 2/2 O(OH)-BO 2/2 (OH)-(OH 0.5 )-PO 2/2 O(OH)]. Fe 3+  is in an octahedral coordination (Fe(O) 2 (OH) 4 ).

zeitschrift für naturforschung b

Fe[B 2 P 2 O 7 (OH) 5 ]: Ein neues Boro-phosphat mit unverzweigten Vierer-Einfach Tetraederketten / Fe[B 2 P 2 O 7 (OH) 5 ]: A New Borophosphate Containing Non-Branched Tetrahedral Vierer-Einfach Chains