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Crown ether complexed pentachloro(aqua)platinic acid, (H 3 O)[PtCl 5 (H 2 O)]·2(18-cr-6)·6H 2 O (1) reacts with glycine, L-alanine, and DL-2-aminobutyric acid to give cis-[PtCl 4 (O-glyH)(H 2 O)]·(18-cr-6)·H 2 O (4a) 1  and cis-[PtCl 4 (O-amacH)(H 2 O)]·(18-cr-6) (amacH = alaH 4b, abuH 4c), respectively, as well as (amacH 2 ) 2 [PtCl 6 ]·2(18-cr-6) (amacH = glyH 5a, alaH 5b, abuH 5c). The crown ether complexed hexachloroplatinic acid, (H 3 O) 2[PtCl 6 ]·2(18-cr-6) (2), reacts with glycine to afford (glyH 2 )[PtCl 4 (N,O-gly)]·2(18-cr-6)·1.25H 2 O (6).

zeitschrift für naturforschung b

Synthese und Charakterisierung von kronenetherstabilisierten Platin(IV)- Komplexen mit Aminosäureliganden / Synthesis and Characterization of Amino Acid Complexes of Platinum(IV) Stabilized by Crown Ethers