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By treatment of [Pt(ox) 2 ] 2-  with hydrogen peroxide the octahedral trans-[Pt(OH) 2 (ox) 2 ] 2-  is formed. From the saturated aqueous solution in the presence of dipyridiniomethane dications single crystals of the double complex salt trans-(py 2 CH 2 )[Pt(OH) 2 (ox) 2 ] trans-(py 2 CH 2 )[Pt(OH)(ox) 2 (H 2 O)] 2 ·  4H 2 O were grown and an X-ray structure determination (tricli­nic, space group P1̄, a = 8.649(1), b = 11.189(3), c = 12.731 (2) Å, α = 79.075(12), β = 80.725(8), γ= 73.932(13)°, Z = 1) has been performed. The centrosymmetric trans-[Pt(OH) 2 (ox) 2 ] 2-  is connected via hydrogen bonds between its hydroxide groups and the aqua ligands of two protonated complex anions trans-[Pt(OH)(ox) 2 (H 2O )] -  .

zeitschrift für naturforschung b

Kristallstruktur des Doppelkomplexsalzes trans-(py 2 CH 2 )[Pt(OH) 2 (ox) 2 ]transs-(py 2 CH 2 )[Pt(OH)(ox) 2 (H 2 O)] 2 ·4H 2 O / Crystal Structure of the Double Complex Salt trans-(py 2 CH 2 )[Pt(OH) 2 (ox) 2 ](H 2 O)] 2 ·4H 2 O