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Black-red single crystals of [Me 3 PN(H)PMe 3 ] 4 I 28  have been prepared by the reaction of [Me 3 PNPMe 3 ]I with iodine in dichloromethane solution in the presence of Me 3 SiI and traces of water. The polyiodide crystallizes triclinically in the space group P1̄ with two formula units per unit cell with the lattice dimensions a = 831.2(1), b = 1661.2(3), c = 1739.0(3) pm, α = 87.26(1)°, β = 79.48(1)°, γ = 78.17(1)°. The structure consists of [Me 3 PN(H)PMe 3 ] 2+  ions, linear I 3-  ions, z-shaped I8 2-  ions, and zig-zag chains of I 14  4-  ions, the terminal iodine atoms of which form I···H-N hydrogen bridges to the cations.

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Die Kristallstruktur von [Me 3 PN(H)PMe 3 ] 4 l 28 , einem Polyiodid mit I 3- -, l8 2- - und I 14  4- -Ionen Crystal / Structure of [Me 3 PN(H)PMe 3 ] 4 I 28 , a Polyiodide with I 3- , I 8  2-  , and I  14  4-  Ions