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By reaction of K 3 [Os(NCS) 3 (SCN) 3 ] with pyridine and glycerine the complex mer- [Os(NCS) 3 Py 3 ] is formed. The X-ray structure determination on a single crystal (monoclinic, space group C2/c, a = 18.6156(12), b = 15.9448(7), c = 19.555(2) Å, β = 94.657(7)°, Z = 8) reveals that the nearly linear thiocyanate groups are exclusively bonded via the N atoms with Os-N-C angles ranging from 169.9° to 177.7°.

Darstellung und Kristallstruktur von /wer-[Os(NCS) 3 Py 3 ] / Synthesis and Crystal Structure of mer-[Os(NCS) 3 Py 3 ]