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By reaction of [B 6 H 6 ] 2-  with (PPh 3 ) 3 AgCl in dichloromethane the belt-shaped hypho-hexaborane adduct [(PPh 3 ) 2 B 6 H 10 ] is formed. The crystal structure of [(PPh 3 ) 2 B 6 H 10 ]·CH 2 Cl 2  has been determined by single crystal X-ray diffraction analysis: orthorhombic, space group Pbnb with a = 9.804(3), b = 17.864(4), c = 21.334(2) Å, Z = 4.

zeitschrift für naturforschung b

Darstellung und Kristallstruktur von Bis(triphenylphosphin)-decahydro-hypho-hexaboran [(PPh 3 ) 2 B 6 H 10 ]·CH 2 Cl 2  / Synthesis and Crystal Structure of Bis(triphenylphosphine)-decahydro-hypho-hexaborane[( PPh 3 ) 2 B 6 H 10 ]CH 2 Cl 2