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Hydrolysis of gallium tribromide complexes of 1,2-bis(diphenylphosphino)benzene in toluene solvent affords crystals of the mono-phosphonium salt [ 1,2 -Ph 2 P-(C 6 H 4 )-PPh 2 H] +  [GaBr 4 ] -  . The structure analysis by single crystal X-ray diffraction allows an internal comparison of Ph 2 P phosphino and Pf 2 PH +  phosphonium functions.

Isolation and Structural Characterisation of Monoprotonated 1,2-Bis(diphenylphosphino)benzene in its Tetrabromogallate(III) Salt