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The reaction between Br 3 GeAll (1) and N(CH 2 CHMeOSnBu 3 ) 3  (2, mixture of isomers) yielded N(CH 2 CHMeO) 3 GeAll (3) as a mixture of diastereomers. Three azagermatranes of the type N(CH 2 CH 2 NR) 3 GeAll (9, R = H; 10, R = Me; 11, R = Me 3 Si) have been synthesized from the reaction of (Me 2 N) 3 GeAll (5) with N (CH 2 CH 2 NHR) 3  (R = H, 6; Me, 7; Me 3 Si, 8). Composition and structures of the new compounds were established by elemental analyses,  1 H and  13 C NMR spectroscopy and mass spectrometry.

Synthesis and Characterization of 1-Allyl-3,7,10-trimethylgermatrane and 1-Allylazagermatranes