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The formation of mixed-ligand complexes of the type [Re Vl NCl 4-n F n ] -  (n = 1 -3) during the reaction of [Re VI NCl 4 ] -  with [n-(C 4 H 9 ) 4 N]F, KF, and HF is reported. Evidence of the individual mixed-ligand compounds is given by their EPR spectral data. In frozen solutions a specific dependence of the EPR data on the composition of the coordination sphere could be detected. This is shown (i) by a nearly linear dependence of g II  and A II  Re on the Cl/F-content of the [Re VI NCl 4-n F n ] -  unit (additivity rules) and (ii) by well-resolved  19 F hyperfine splittings.

zeitschrift für naturforschung b

Zur Existenz von [ReNCl 4-n F n ] -  (n = 1-3) Nitridorhenat(VI)-Gemischt- ligandkomplexen -Eine EPR-Untersuchung / EPR Evidence of [ReNCl 4-n  F n J –  (n = 1-3) Nitridorhenate(VI) Mixed-Ligand Complexes