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Starting from HoSe 2-x  powder and holmium metal bright brownish-yellow, plate-like single crystals of Ho 2 Se 3  could be prepared by chemical transport with AlCl 3 . Holmium sesquiselenide crystallizes in the Sc 2 S 3 -type structure, space group Fddd, with lattice constants a = 1140,7(2), b -812,6(1) and c = 2423,9(3) pm.

Zur Kristallstruktur von Ho 2 Se 3 / On the Crystal Structure of Ho 2 Se 3