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By reaction of [B 6 H 6 H fac ] -  with cobaltocene in acetonitrile [(C 5 H 5 )Co(C 5 H 4 )B 6 H 5 H fac ] is formed. Its crystal structure has been determined by single crystal X-ray diffraction analysis (monoclinic, space group P2 1 /n with a = 9.786(2), b = 9.726(2), c = 13.938(2) A, β = 107.2850(3)°, Z = 4). The B 6  octahedron is slightly compressedoin the direction of the B-C bond by about 1%, with B-B bond lengths between 1.69 and 1.87 A. The  11 B NMR spectrum exhibits a 1:4:1 pattern of a monosubstituted B 6  cage. In the IR and Raman spectra characteristic B-H vibrations are observed.

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Darstellung, spektroskopische Charakterisierung und Kristallstruktur von Dicyclopentadienylcobalt-hexahydro-closo-hexaborat [(C 5 H 5 )Co(C 5 H 4 )B 6 H 5 H fac ]/ Synthesis, Spectroscopic Characterization and Crystal Structure of Dicyclopentadienyl- cobalt-hexahydro-closo-hexaborate [(C 5 H 5 )Co(C 5 H 4 )B 6 H 5 H fac ]