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A new fullerene co-crystal C 60 *SiH(C 6 H 5 ) 3  has been synthesized by crystallisation from a melt of SiH(C 6 H 5 ) 3  and C 60  in sealed duran tubes at 80°C. X-ray investigations led to triclinic symmetry, space group P1̄, a = 10.086(1), b = 14.431(2), c = 14.911(2) Å, α = 79.13(1), β = 74.943(9), γ = 88.33(1)°, V = 2058.0(4) Å 3 , Z = 2. The crystal structure consists of isolated fullerene and silane molecules. At -80°C, C 60  is still rotationally disordered. Temperature dependent Guinier powder diagrams do not show any phase transformation between 25 and -165°C. The compound is stable in air.

zeitschrift für naturforschung b

Synthese und Charakterisierung des Fulleren-Kokristallisats C 60 *SiH(C 6 H 5 ) 3 /Synthesis and Characterisation of the Fullerene Co-Crystal C 60 *SiH(C 6 H 5 ) 3