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The isotypic borophosphates Rb[B 2 P 2 O 8 (OH)] and Cs[B 2 P 2 O 8 (OH)] were grown under hydrothermal conditions. The crystal structures were solved by single crystal methods (Rb[B 2 P 2 O 8 (OH)]/ Cs[B 2 P 2 O 8 (OH)]: monoclinic, P2 1 /c, a = 676.2(3)/682.7(3), b = 1217.3(5)/ 1236.8(5), c = 885.0(4)/900.6(5) pm, β = 97.3(1)/ 98.1(1)°. Z = 4). The structures contain a complex framework of three-, four-, six-, nine- and twelvemembered rings of tetrahedra. Along [100] the twelve-membered rings are stacked to give wide channels which contain the Rb + /Cs + -ions in an icosahedral coordination.

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Rb[B 2 P 2 O 8 (OH)] und Cs[B 2 P 2 O 8 (OH )]: Die ersten Borophosphate mit dreidimensional vernetzter Anionenteilstruktur  /Rb[B 2 P 2 O 8 (OH)] and Cs[B 2 P 2 O 8 (OH )]: The First Borophosphates with a Threedimensional Anionic Tetrahedral Structure