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Yellow single crystals of the isotypic phases Ca 51 [WN 4 ] 12 N 8 O 3  and Sr 51 [WN 4 ]  12 N 8 O 3  (triclinic, P1̄ (#2 ); a= 1056.4(3) / 1113.1(5) pm, b = 1239.7(3) / 1304.4(5) pm, c= 1598.2(3) / 1679.4(9) pm, α = 102.78(1)/102.47(2)°, β= 95.15( 1)/95.43(3)°, γ = 109.89(1)/109.77(2)°; Z = 1) were grown in a Tl-flux (Ca:Tl, molar ratio 5:1, W-crucible; T max  = 1273K; reaction with N 2 , 1 atm, 36 h) or from pellets (Sr 2 N + W, molar ratio 6:1; T max  = 1023K; reaction with N 2 , 1 atm, 36 h). The crystal structures contain tetrahedral anions [WN 4 ] 6-  in addition to isolated nitride and isolated oxide ions, which are octahedrally coordinated by Ca and Sr, respectively.

zeitschrift für naturforschung b

Die Kristallstrukturen der isotypen Erdalkalimetall-Nitridowolfra- mat(VI)-Nitrid-Oxide Ca 51 [WN 4 ] 12 N 8 O 3  und Sr 51 [WN 4 ] 12 N 8 O 3  / The Crystal Structures of the Isotypic Alkaline Earth-Nitridotungstate(VI)- Nitride-OxidesCa 51 [WN 4 ] 12 N 8 O 3  and Sr 51 [WN 4 ] 12 N 8 O 3