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The reactions of benzo-18-crown-6 with MeX 2  (Me = Cd, Hg; X = Cl. Br), and of dibenzo-18-crown-6 with Hg(CN) 2  afford the compounds [Me(benzo-18-crown-6)X 2 ] (1-4) and [Hg(dibenzo-18-crown-6)(CN) 2  (5), resp., the crystal structures of which were determined. They consist of isolated neutral molecules, the crystalline Cd complexes and 5 contain one molecule of water of crystallization per formula unit, which however is not coordinated to the metal atom. The metal atoms are coordinated by the six O atoms of the ligands and the two halide atoms, or the two CN groups for 5, resp., the coordination being more unsymmetrical for the benzo than for the dibenzo ligand.

zeitschrift für naturforschung b

Reaktionen von Cadmium-und Quecksilber(II)halogeniden und -pseudohalogeniden mit Kronenethern: Kristallstrukturen der Komplexe von Benzo-18-krone-6 mit CdX 2  und HgX 2  (X = CI, Br) und von Dibenzo-18-krone-6 mit Hg(CN) 2  / Reactions of Cadmium and Mercury(II) Halides and Pseudohalides with Crown Ethers: Crystal Structures of the Complexes of Benzo-18-crown-6 with CdX 2  and HgX 2  (X = Cl, Br) and of Dibenzo-18-crown-6 with Hg(CN) 2