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The solid-state structures of the low-melting compounds bis(trifluoromethyl)disulfane (CF 3 SSCF 3 , triclinic, space group P 1̄, Z = 2) and bis(trifluoromethyl)trisulfane (CF 3 SSSCF 3 , monoclinic, space group C2/c, Z = 4) have been determined on single crystals with MoK α radiation at -160°C. The trisulfane has trans conformation. The geometry of both molecules agrees well with results of electron diffraction on the gaseous state. A comparison is made also with the crystal structures of the related molecules CF 3 TeTeCF 3  and CF 3 OOOCF 3

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Bis(trifluormethyl)disulfan und -trisulfan: Molekülgeometrie im festen Zustand [1]  / Bis(trifluoromethyl)disulfane and Trisulfane: Molecular Geometry in the Solid State [1]