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[Mo(NPMe 3 ) 4 ]Cl 2  has been prepared by the reaction of MoNCl 3  with N-(trimethylsilyl)trimethylphosphanimine in dichloromethane solution from which the complex crystallizes with one CH 2 Cl 2  molecule per formula unit. [Mo(NPMe 3 ) 4 ]Cl 2 ·CH 2 Cl 2 : Space group P2 1 /c, Z = 4. Lattice dimensions at-40°C : a = 1244.2( 1), b = 1609.6(1), c = 1595.9( 1) pm, β = 90.36( 1)°. The structure consists of chloride ions and dications [Mo(NPMe 3 ) 4 ] 2+  in which the molybdenum atom is tetrahedrally coordinated by the four nitrogen atoms of the (NPMe 3 ) -  groups with MoN bond lengths of 180.7 pm in average which correspond with double bonds.

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Tetrakis(trimethylphosphaniminato)molybdän-dichlorid, [Mo(NPMe 3 ) 4 ]Cl 2  / Tetrakis(trimethylphosphoraneiminato)molybdenum Dichloride, [Mo(NPMe 3 ) 4 ]Cl 2